FlowSorb III
Dynamic Sorption Surface Area Analyzer
- Precise and high speed surface area analysis.
- 在一种仪器中包括准备和分析仪
- Suitable for a wide variety of surface area measurements
Flowsorb III以速度,准确性和可靠性提供单点和多点BET表面积测量。很容易容纳具有从0.01 m2 /g到1,000 m2 /g的表面积的样品。
Features and Benefits:
- 超稳定的检测器消除了漂移和恒定调整的需求
- Cold trap conveniently located in front vs. side placement, as in other instruments. This placement reduces the chance of breakage.
- Single injection calibration requires only one control setting. Adaptable to any non-corrosive adsorbate mix.
- All controls and displays are at eye/ arm level, out of the spill zone
- Built-in sample preparation Rugged construction for day-in, dayout operation
- 崎rugged的施工,用于日间运营
规格s
Applicability
| Surface Area | 0.1 m² (minimum); 280平方米(最大) |
| 特定的表面积 | Approximately 0.01 m²/g (minimum) |
准确性& Reproducibility
| 低比表面 | Typically better than ±3% (single point method) ±2% (multipoint method) reproducibility within ±0.5% |
| Moderate-to-High Specific surfaces | 通常好于±2%(单点方法) ±1.5% (multipoint method) reproducibility within ±0.5% |
System Capacity
| 样品支架量 | 4.8cm³; other sizes available |
Physical
| Dimensions | 46.5W x 53h x 30.5d cm(18.3W x 20.9h x 12d in) |
| FlowSorb III 2305 | Weight: 18 kg (40 lbs) |
| FlowSorb III 2310 | 重量:20公斤(44磅 |
Degas System
| 温度范围 | 环境350°C |
| Selection | Digitally set, 1 °C increments |
| 准确性 | 在热电偶处的设定点的偏差小于±10°C |
环境
| 温度 | 15-30°C(59-90°F)运行;0-50°C(32-122°F)存储和运输 |
| Humidity | 20-80% relative (non-condensing |
电气
| 电压 | 100,115,230 VAC±10% |
| Frequency | 50/60Hz |
| Power | 240 VA, operating (maximum) |
Gas
| 氦与氮的混合物,氩气,k,二氧化碳,乙烷,N-丁烷和其他非腐蚀性气体的混合物。30%N的混合物2和70%的人建议单点分析。建议使用HE和大约5、12、18和24%N2的混合物用于多点BET。 |
技术
通过流动气体法进行表面积,涉及在大气压下在样品上的吸附性和惰性气体混合物的连续流动。
The FlowSorb III’s reproducibility is better than 0.5%. The FlowSorb III 2310 features a built-in Dewar elevator for completely automated analysis and rewarming fan for rapidly warming the sample tube to increase the speed of the sample analysis. Single injection calibration provides fast start-up and high sample throughput. Specially designed sample holders can be attached and removed from the instrument with one hand.
These quick connect/disconnects have a built-in isolation valve to prevent sample contamination. The FlowSorb III 2305 features a Dewar support latch system that provides one-handed convenience and safe guards against LN2 spills. Simple in design, the Flow-Sorb III requires minimal training time and leaves little chance of operator error. Automatic mode switching for adsorption and desorption is accomplished without operator attention. The low purchase price of the FlowSorb III and its accessories make this instrument one of the most inexpensive ways for a laboratory to begin measuring BET surface area.
申请说明
标准方法
- ISO 4652 RUBBER COMPOUNDING INGREDIENTS – CARBON BLACK – DETERMINATION OF SPECIFIC SURFACE AREA BY NITROGEN ADSORPTION METHODS – SINGLE-POINT PROCEDURES
- ISO 9277通过气体吸附测定固体的特定表面积 - BET方法
- ASTM D4567标准测试方法,用于使用连续流量法使用氮的吸附来确定催化剂和催化剂载体的特定表面积
- ASTM D5604单点B.E.T.的沉淀二氧化硅表面区域的标准测试方法氮的吸附
- https://www.iso.org/standard/75103.html
- https://www.iso.org/standard/44941.html
- https://www.astm.org/Standards/D4567.htm







